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Dollars Store for the Appleton, WI 54914 at 1218 Letter Badger Ave

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₂O₄ nanoparticles with temperature varying from 500 to 800°C. The two ferrite samples calcined at 500–600°C were obtained as single spinel phase with peaks at 220, 311, 400, 511, and 440, corresponding to the cubic spinel structure (JCPDS card. no. 01-071-1232) . It is showed that the increase in temperature is associated with the improvement of MgFe₂O₄ powders. However, from 700 to 800°C, new phases of ?-Fe₂O₃ were observed. The spinel phase of MgFe₂O₄ was confirmed by five XRD peaks at 220, 311, 400, 511, and 440 crystal planes. Results reported in Table 1 also indicate that the crystallite size of MgFe₂O₄ was positively associated with the calcination temperature. As temperature moved from 500 to 800°C with 100°C interval, the average crystallite size was expanded from 18 to 61 nm. For the “a” lattice parameter, XRD spectra showed that for MgFe₂O₄ nanoparticles, the value fell in the range of 8.344–8.378 A.

The SEM images of different samples of MgFe₂O₄ nanoparticles corresponding to four calcination temperature points of 500°C, 600°C, 700°C, and 800°C are shown in Figures 3(a)–3(d). Visually, the images showed consistent implication with the XRD results. To be specific, particle size of the prepared samples were found to be proportionally increasing with temperature. This could possibly be due to the aggregation and coalescence during desiccation.

The TEM image of MgFe₂O₄ synthesized at 500°C is presented in Figure 4(a). Evidently, the magnesium ferrite nanoparticles resulted from the solution combustion method were uniform in terms of morphology and crystallite size and reached the particle size of approximately 30 nm. Continue reading “Figure 2 displays different X-ray diffraction patterns of MgFe”